Search Thermo Fisher Scientific
Search Thermo Fisher Scientific
Catalog Number | Height (English) | Height (Metric) | Includes |
---|---|---|---|
FISK570035-0250 | 22.04 in. | 56 cm | Hooked model with polyacetal clamps, 250mL flask |
FISK570025-0500 | 23.62 in. | 60 cm | Hooked model with springs, 500mL flask |
Preparation involves filling the flask to between 40 to 60 percent of capacity. To prevent sample loss initially, column should be pre-wet with about 1mL of the solvent used in the concentration. If solvent is allowed to escape, entire assembly should be set up in a hood. Charged assembly should be placed over a vigorously boiling water bath. Water level should be maintained just below the lower joint and apparatus mounted so that the lower rounded surface of the flask is bathed in steam. Final sample remains in the lower tube for further analysis.